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Tinh luyện Rietveld bằng nhiễu xạ tia X (XRD)×Quang phổ photoelectron tia X×
Lĩnh vựcKhoa học vật liệuKhoa học vật liệu
HọProcess / pipelineProcess / pipeline
Năm ra đời19691967
Người khởi xướngHugo RietveldKai Siegbahn
LoạiRefinement methodAnalytical technique
Công trình gốcRietveld, H. M. (1969). A profile refinement method for nuclear and magnetic structures. Journal of Applied Crystallography, 2(2), 65-71. DOI ↗Siegbahn, K., Nordling, C., Fahlman, A., et al. (1967). ESCA: Atomic, Molecular and Solid State Structure Studied by Means of Electron Spectroscopy. Almqvist and Wiksells. link ↗
Tên gọi khácRietveld refinement, powder diffraction refinementXPS, ESCA, electron spectroscopy for chemical analysis
Liên quan33
Tóm tắtXRD Rietveld Refinement is a method for extracting detailed crystal structure information from powder diffraction data by comparing observed and calculated diffraction patterns through least-squares refinement. Developed by Hugo Rietveld in 1969, this technique enables determination of atomic positions, occupancies, thermal parameters, and phase fractions directly from powder data without requiring single crystals. It is the standard approach in materials characterization for structural analysis, phase identification, and quantification.X-ray Photoelectron Spectroscopy (XPS), also known as Electron Spectroscopy for Chemical Analysis (ESCA), is a surface-sensitive analytical technique that measures the kinetic energies of photoelectrons ejected from a material by high-energy X-rays. Developed by Kai Siegbahn in 1967, XPS determines elemental composition, chemical oxidation states, and chemical bonding within ~10 nanometers of a surface. It is indispensable in materials science for surface characterization, corrosion studies, oxide analysis, and interface chemistry.
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ScholarGateSo sánh phương pháp: XRD Rietveld Refinement · X-ray Photoelectron Spectroscopy. Truy cập ngày 2026-06-19 từ https://scholargate.app/vi/compare