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Refinamiento Rietveld de DRX×Espectroscopia fotoelectrónica de rayos X×
CampoCiencia de materialesCiencia de materiales
FamiliaProcess / pipelineProcess / pipeline
Año de origen19691967
Autor originalHugo RietveldKai Siegbahn
TipoRefinement methodAnalytical technique
Fuente seminalRietveld, H. M. (1969). A profile refinement method for nuclear and magnetic structures. Journal of Applied Crystallography, 2(2), 65-71. DOI ↗Siegbahn, K., Nordling, C., Fahlman, A., et al. (1967). ESCA: Atomic, Molecular and Solid State Structure Studied by Means of Electron Spectroscopy. Almqvist and Wiksells. link ↗
AliasRietveld refinement, powder diffraction refinementXPS, ESCA, electron spectroscopy for chemical analysis
Relacionados33
ResumenXRD Rietveld Refinement is a method for extracting detailed crystal structure information from powder diffraction data by comparing observed and calculated diffraction patterns through least-squares refinement. Developed by Hugo Rietveld in 1969, this technique enables determination of atomic positions, occupancies, thermal parameters, and phase fractions directly from powder data without requiring single crystals. It is the standard approach in materials characterization for structural analysis, phase identification, and quantification.X-ray Photoelectron Spectroscopy (XPS), also known as Electron Spectroscopy for Chemical Analysis (ESCA), is a surface-sensitive analytical technique that measures the kinetic energies of photoelectrons ejected from a material by high-energy X-rays. Developed by Kai Siegbahn in 1967, XPS determines elemental composition, chemical oxidation states, and chemical bonding within ~10 nanometers of a surface. It is indispensable in materials science for surface characterization, corrosion studies, oxide analysis, and interface chemistry.
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ScholarGateComparar métodos: XRD Rietveld Refinement · X-ray Photoelectron Spectroscopy. Recuperado el 2026-06-19 de https://scholargate.app/es/compare