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Powierzchnia właściwa BET×Analiza Termograwimetryczna×Rafinacja Rietvelda metodą XRD×
DziedzinaInżynieria materiałowaInżynieria materiałowaInżynieria materiałowa
RodzinaProcess / pipelineProcess / pipelineProcess / pipeline
Rok powstania19381960s1969
TwórcaBrunauer, Emmett, TellerWilliam W. WendlandtHugo Rietveld
TypMeasurement methodCharacterization methodRefinement method
Źródło pierwotneBrunauer, S., Emmett, P. H., & Teller, E. (1938). Adsorption of gases in multimolecular layers. Journal of the American Chemical Society, 60(2), 309-319. DOI ↗Wendlandt, W. W. (1986). Thermal Analysis (3rd ed.). John Wiley & Sons. link ↗Rietveld, H. M. (1969). A profile refinement method for nuclear and magnetic structures. Journal of Applied Crystallography, 2(2), 65-71. DOI ↗
Inne nazwyBET analysis, nitrogen adsorption, surface area measurementTGA, thermal gravimetry, thermogravimetryRietveld refinement, powder diffraction refinement
Pokrewne333
PodsumowanieBrunauer-Emmett-Teller (BET) Surface Area Analysis is a technique for measuring the specific surface area of solids by analyzing their nitrogen adsorption isotherms. Developed by Brunauer, Emmett, and Teller in 1938, BET theory extends monolayer adsorption (Langmuir) to multilayer adsorption, enabling quantification of surface area of porous and powdered materials. It is the industry standard for characterizing catalysts, adsorbents, pharmaceuticals, and porous materials, providing critical data for performance prediction and quality control.Thermogravimetric Analysis (TGA) is a thermal characterization technique that continuously measures mass loss or gain of a material as a function of temperature (or time at constant temperature). Developed systematically by William Wendlandt and colleagues in the 1960s, TGA identifies thermal transitions (evaporation, decomposition, oxidation, reduction) and quantifies composition of polymers, pharmaceuticals, ceramics, and other materials. The derivative signal (DTG) highlights transition temperatures. When combined with gas analysis (MS, FTIR), decomposition products are identified.XRD Rietveld Refinement is a method for extracting detailed crystal structure information from powder diffraction data by comparing observed and calculated diffraction patterns through least-squares refinement. Developed by Hugo Rietveld in 1969, this technique enables determination of atomic positions, occupancies, thermal parameters, and phase fractions directly from powder data without requiring single crystals. It is the standard approach in materials characterization for structural analysis, phase identification, and quantification.
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ScholarGatePorównaj metody: BET Surface Area · Thermogravimetric Analysis · XRD Rietveld Refinement. Pobrano 2026-06-19 z https://scholargate.app/pl/compare